Project #36664 - Resolution of a Phenylethylamine

Make direct comparisons: If your values are lower than the typical values, briefly gives possible reasons for such an occurrence.

A) Experimental yield vs. typical yield

b) Experimental specific rotation vs. typical specific rotation.

 

grams of phenylethylamine: 10.6 ml (in 75 l methanol)

g of tartaric acid: 12.47 g

mass of organic compound before decantation: 27.013g

mass of organic compound after decantation: 1.578 g

-2.9 left degree of rotation S [a]d= -15

optical purity: 37%

S Enantiomer: 69 %

R Enantiomer 31%

 

melting point: 169.0-171.0 i need to answer the 2 previous questions and also write a disscussion about the experiment that I did analyzing my results and why I obtained them, explaining what I did in detail. I will provide pictures of the procedures. 

i ned

Subject Science
Due By (Pacific Time) 07/29/2014 02:00 pm
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