Project #65242 - ochem pre-lab

YOU ONLY NEED 1)THE THE TABLE FOR REACTANTS AND PRODUCTS FOR THE FORMATION OF THE YLID AND 2) THE TABLE FOR THE SOLVENTS ETC FOR THAT STEP.

 

Lab 11 Preparation of the Phosphonium Salt Procedure

 You will need this salt to run the Wittig reaction next week. The yield is very low so we will pool each student mixture into a class sample and reflux that sample for one week.

In a 25 mL erlenmeyer charged with a stir bar, combine 1.31 g of triphenylphosphine, 6 mL of toluene, and 0.7 mL of p-methylbenzyl chloride. Stir until dissolution is complete. Give your sample to your TA who will set up a class reflux and reflux the sample for one week.

 

Subject Science
Due By (Pacific Time) 04/05/2015 08:00 pm
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